[1]刘青,邓毅,南建理,等.HPLC法测定复方麻桂喷雾剂中桂皮醛含量[J].甘肃中医药大学学报,2007,(06):39-41.
 Liu Qing,Deng Yi,Nan Jianli,et al.Determination of the content of cinnamic aldehyde in compound Magui Spray by HPLC[J].Journal of Gansu University of Chinese Medicine,2007,(06):39-41.
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HPLC法测定复方麻桂喷雾剂中桂皮醛含量()
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《甘肃中医药大学学报》[ISSN:1003-8450/CN:62-1062/R]

卷:
期数:
2007年06期
页码:
39-41
栏目:
中药研究
出版日期:
1900-01-01

文章信息/Info

Title:
Determination of the content of cinnamic aldehyde in compound Magui Spray by HPLC
作者:
刘青1 邓毅1 南建理2 宁艳梅1
1. 甘肃中医学院, 甘肃 兰州 730000;
2. 甘肃省药物研究所, 甘肃 兰州 730000
Author(s):
Liu Qing1 Deng Yi1 Nan Jianli2 Ning Yanmei1
1. Gansu College of TCM, 730000, Lanzhou, China;
2.Gansu Research Institute of Medicines, 730000, Lanzhou, China
关键词:
HPLC复方麻桂喷雾剂桂皮醛
Keywords:
HPLCcompound Magui Spraycinnamic aldehyde
分类号:
R284.1
摘要:
目的 探索复方麻桂喷雾剂中桂皮醛的含量测定方法。方法 采用甲醇提取样品;Hypersil ODS-2柱(250 mm×4.6 mm,5 μm);流动相:乙腈-水(30:70);检测波长290 nm。结果 线性范围为13.9~139.04 μg/mL(r=0.9992),平均回收率为100.3%,RSD为2.17%。结论 该方法简便、快速、准确,可用于复方麻桂喷雾剂中桂皮醛含量的测定。
Abstract:
Objective To research the determining method of the content of cinnamic aldehyde in compound Magui Spray. Methods Extracted the specimen with methanol. Hypersil ODS-2 column (250 mm×4.6 mm,5 μm) was used.Mobile phase consisted of acetonitrile-water (30:70). The detection wavelength was 290 nm.Results The linear rang was from 13.9 to 139.04 μg/mL(r=0.9992), the average recovery was 100.3%,RSD was 2.17%.Conclusion The method is handy,fast and accurate,and it is suitable for the quality control of compound MaGui Spray.

参考文献/References:

[1] 国家药典委员会.中华人民共和国药典[M].北京:化学工业出版社,2005:91.

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备注/Memo

备注/Memo:
收稿日期:2006-10-19;改回日期:2007-04-03。
作者简介:刘青(1976-),男,在读硕士研究生。研究方向:中药的性能与临床研究。
更新日期/Last Update: 1900-01-01